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Our Publications

List of peer-reviewed research articles, reviews, book chapters and other contributions.

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2024

68-Characterization of a mixed mode fluorocarbon/weak anion exchange sorbent for the separation of perfluoroalkyl substances

A A Olomukoro, R Xie, F X Fernandez Paucar, C DeRosa, N D Danielson, E Gionfriddo

Journal of Separation Science 47 (16), 2400413

67-Green and sustainable evaluation of methods for sample treatment in drug analysis

H Martínez-Pérez-Cejuela, E Gionfriddo, P Campíns-Falcó, JM Herrero-Martínez, S. Armenta

Green Analytical Chemistry 10, 100125

66-Evolution of Green Sample Preparation: Fostering a Sustainable Tomorrow in Analytical Sciences

​H Martínez-Pérez-Cejuela, E Gionfriddo

Analytical Chemistry 96 (20), 7840-7863

2023

65-Enhancing Quantitative Analysis of Xenobiotics in Blood Plasma through Cross-Matrix Calibration and Bayesian Hierarchical Modeling

NH Godage, SS Qian, E Cudjoe, E Gionfriddo

ACS Measurement Science Au 4 (1), 127-135

 

64-ExTech 2023, Celebrating 25 Years of Innovation in Extraction Technologies

E Gionfriddo

LCGC NORTH AMERICA 41 (11), 479-479

63-Matrix effects demystified: Strategies for resolving challenges in analytical separations of complex samples

​ML Williams, AA Olomukoro, RV Emmons, NH Godage, E Gionfriddo

Journal of Separation Science 46 (23), 2300571

62Quantitative determination of pesticides in human plasma using bio-SPME-LC–MS/MS: a robust tool to assess occupational exposure to pesticides

​NH Godage, E Cudjoe, T Chau, E Gionfriddo

Analytical and Bioanalytical Chemistry 415 (18), 4423-4434

61Investigation of the adsorption/desorption mechanism of perfluoroalkyl substances on HLB-WAX extraction phases for microextraction

AA Olomukoro, C DeRosa, E Gionfriddo

Analytica Chimica Acta 1260, 341206

 

60Rapid Screening and Quantification of PFAS Enabled by SPME-DART-MS

RV Emmons, W Fatigante, AA Olomukoro, B Musselman, E Gionfriddo

Journal of the American Society for Mass Spectrometry

 

59- Practical Aspects for SPME Method Development in Complex Samples

A Kasperkiewicz, S Lendor, E Gionfriddo

In Evolution of Solid Phase Microextraction Technology (pp. 32-74). The Royal Society of Chemistry

58Design and Preclinical Evaluation of Nicotine–Stearic Acid Conjugate-Loaded Solid Lipid Nanoparticles for Transdermal Delivery: A Technical Note

J Renukuntla, S Peterson-Sockwell, BA Clark, NH Godage, E Gionfriddo

Pharmaceutics 15 (4), 1043

57Automated method using direct-immersion solid-phase microextraction and on-fiber derivatization coupled with comprehensive two-dimensional gas chromatography high-resolution mass spectrometry for profiling naphthenic acids in produced water

J Crucello, NMFM Sampaio, IM Junior, RM Carvalho, E Gionfriddo, P Marriott, LW Hantao

Journal of Chromatography A 1692, 463844

56Chapter 5 - Sample preparation in a green perspective

Orfeas-Evangelos Plastiras, Emanuela Gionfriddo, Victoria F. Samanidou

Analytical and Bioanalytical Chemistry, 2023, 1-12

55Threshold Concepts in Analytical Chemistry

MJ Claus, J Monahan, RJ Whelan, MF VithaE Gionfriddo

Green Approaches for Chemical Analysis, 2023, 151-172

2022

54- Leveraging multi-mode microextraction and liquid chromatography stationary phases for quantitative analysis of neurotoxin β-N-methylamino-L-alanine and other non-proteinogenic amino acids

RV Emmons, E Karaj, E Cudjoe, DS Bell, LMV Tillekeratne, E Gionfriddo

Journal of Chromatography A 1685, 463636

 

53Sample preparation in a green perspective

OE Plastiras, E Gionfriddo, VF Samanidou

Green Approaches for Chemical Analysis, 151-172

 

52- Mentorship in the Time of Covid-19: Finding the Silver Lining

E Gionfriddo

LC GC NORTH AMERICA 40 (6), 274-274

51Biocompatible SPME coupled to GC/MS for analysis of xenobiotics in blood plasma

NH Godage, E Gionfriddo

Journal of Chromatography B, 123308

50Unraveling the Complex Composition of Produced Water by Specialized Extraction Methodologies

RV Emmons, GS Shyam Sunder, T Liden, KA Schug, TY Asfaha, JR Kirchhoff, E Gionfriddo*

Environmental Science & Technology

2021

49Ion Exchange Solid Phase Microextraction coupled to Liquid Chromatography/Laminar Flow Tandem Mass Spectrometry for the Determination of Perfluoroalkyl Substances in Water Samples

AA Olomukoro, RV Emmons, NH Godage, E Cudjoe, E Gionfriddo*

Journal of Chromatography A, 462335

48Minimizing transient microenvironment-associated variability for analysis of environmental anthropogenic contaminants via ambient ionization

RV Emmons, E Gionfriddo*

Science of The Total Environment 775, 145789

47-Direct immersion thin film solid phase microextraction of polychlorinated n-alkanes in cod liver oil

D Gruszecka, J Grandy, E Gionfriddo, V Singh, J Pawliszyn

Food Chemistry 353, 129244

 

46-In vivo analytical techniques facilitated by contemporary materials

NH Godage, AA Olomukoro, RV Emmons, E Gionfriddo*

TrAC Trends in Analytical Chemistry, 116290

2020

45- Analysis of food samples made easy by microextraction technologies directly coupled to mass spectrometry

E Gionfriddo, GA Gómez‐Ríos

Journal of Mass Spectrometry  2020;e4665

44Green analytical solutions for sample preparation: solid phase microextraction and related techniques

E Gionfriddo

Physical Sciences Reviews 5 (8)

43Application of in vivo solid phase microextraction (SPME) in capturing metabolome of apple (Malus× domestica Borkh.) fruit

S Risticevic, EA Souza-Silva, E Gionfriddo, JR DeEll, J Cochran, W S Hopkins, J Pawliszyn

Scientific reports 10 (1), 1-11

42- Biocompatible SPME fibers for direct monitoring of nicotine and its metabolites at ultra-trace concentration in rabbit plasma following the application of smoke cessation formulations

NH Godage, E Cudjoe, R Neupane, SHS Boddu, PK Bolla, J Renukuntla, E Gionfriddo

Journal of Chromatography A, 461333

 

41Biocompatible Microextraction Devices for Simple and Green Analysis of Complex Systems

E Gionfriddo

LC-GC North America - Vol. 38 Number s6 June 2020

 

40- Development of Alternative Green Sample Preparation Techniques

E Gionfriddo

Separations 7 (2), 31

 

39- Use of natural sorbents as alternative and green extractive materials: A Critical Review

NH Godage, E Gionfriddo

Analytica Chimica Acta

38-Optimization of thin film solid phase microextraction and data deconvolution methods for accurate characterization of organic compounds in produced water

RV Emmons, T Liden, KA Schug, E Gionfriddo

Journal of Separation Science, 2020

37-Blue light-triggered photochemistry and cytotoxicity of retinal

K Ratnayake, JL Payton, ME Meger, NH Godage, KK Rajanayake, D Isailovic, E Gionfriddo, A Karunarathne

Cellular Signalling 69, 109547

36- Solid phase microextraction coating

JB Pawliszyn, E Gionfriddo, E Boyaci

US Patent 10,545,077

 

35Direct-immersion SPME in soy milk for pesticide analysis at trace levels by means of a matrix-compatible coating

E Gionfriddo, D Gruszecka, X Li, J Pawliszyn

Talanta, 2020, 211, 120746

 

2019

34Development, optimization and applications of thin film solid phase microextraction (TF-SPME) devices for thermal desorption: A comprehensive review

RV Emmons, R Tajali, E Gionfriddo

Separations 6 (3), 39

 

33- Development and validation of a fully automated solid phase microextraction high throughput method for quantitative analysis of multiresidue veterinary drugs in chicken tissue

A Khaled, E Gionfriddo, V Acquaro Jr, V Singh, J Pawliszyn

Analytica chimica acta 1056, 34-46

 

32Exploring the Efficiency of Various Extraction Approaches for Determination of Crude (4-methylcyclohexyl) methanol (MCHM) Constituents in Environmental Samples

RV Emmons, AM Devasurendra, NH Godage, E Gionfriddo

LC GC NORTH AMERICA 37 (4), 28-+

31-Fast screening of illicit drugs in beverages and biological fluids by direct coupling of thin film microextraction to dielectric barrier discharge ionization-mass spectrometry

MF Mirabelli, E Gionfriddo, J Pawliszyn, R Zenobi

Analyst, 2019, 144, 2788-2796

30Recent developments and applications of solid phase microextraction as a sample preparation approach for mass-spectrometry-based metabolomics and lipidomics

N Reyes-Garcés, E Gionfriddo

TrAC Trends in Analytical Chemistry- 113, 172-181

 

29A critical outlook on recent developments and applications of matrix compatible coatings for Solid Phase Microextraction

NH Godage, E Gionfriddo

TrAC Trends in Analytical Chemistry 2019 - 111, 220-228

 

2018

28- Development and Validation of a Fully Automated Solid-Phase Microextraction High Throughput Method for Quantitative Analysis of Multiresidue Veterinary Drugs in Chicken Tissue

A Khaled, E Gionfriddo, V Acquaro Jr, V Singh, J Pawliszyn

Analytica Chimica Acta - 1056, 34-46

 

27Development and Validation of Eco-Friendly Strategies based on Thin Film Microextraction for Water Analysis

H. Piri-Moghadam, E Gionfriddo, J. J.Grandy, Md. N. Alam, J Pawliszyn

Journal of Chromatography A - 1579, 20-30

 

26- Exploiting the tunable selectivity features of polymeric ionic liquid-based SPME sorbents in food analysis

E Gionfriddo, ÉA Souza-Silva, TD Ho, JL Anderson, J Pawliszyn

Talanta 188 (2018) 522–530

25- Direct Immersion Solid-Phase Microextraction Analysis of Multi-class Contaminants in Edible Seaweeds by Gas Chromatography-Mass Spectrometry

L Zhang, E Gionfriddo, V Acquaro, J Pawliszyn

Analytica Chimica Acta 1031(2018)83e9

 

24- Investigating the robustness and extraction performance of a matrix‐compatible solid‐phase microextraction coating in human urine and its application to assess 2–6‐ring polycyclic aromatic hydrocarbons using GC–MS/MS

A Naccarato, E Gionfriddo, R Elliani, J Pawliszyn, G Sindona, A Tagarelli

Journal of Separation Science 41 (4), 929-939

 

23- A quantitative approach for pesticide analysis in grape juice by direct interfacing of a matrix compatible SPME phase to dielectric barrier discharge ionization-mass spectrometry

MF Mirabelli, E Gionfriddo, J Pawliszyn, R Zenobi

Analyst 143 (4), 891-899

 

22- Advances in solid phase microextraction and perspective on future directions

N Reyes-Garcés, E Gionfriddo, GA Gómez-Ríos, MN Alam, E Boyacı, B Bojko, V Singh, J Grandy, J Pawliszyn

Analytical Chemistry 90 (1), 302-360

2017

Solid phase microextraction coating

JB Pawliszyn, E Gionfriddo, E Boyaci

US Patent App. 15/446,972

 

21- Complex Matrices Analysis by Direct-Immersion SPME with Matrix-Compatible Coatings: A New Approach Compatible with Automation

J Pawliszyn, E Gionfriddo

LC GC NORTH AMERICA 35 (8), 519-521

 

20- Ultrafast Screening and Quantitation of Pesticides in Food and Environmental Matrices by Solid-Phase Microextraction–Transmission Mode (SPME-TM) and Analysis in Real Time (DART)

GA Gómez-Ríos, E Gionfriddo, J Poole, J Pawliszyn

Analytical Chemistry 89 (13), 7240-7248

 

19- A new and efficient Solid Phase Microextraction approach for analysis of high fat content food samples using a matrix-compatible coating

S De Grazia, E Gionfriddo, J Pawliszyn

Talanta 167, 754-760

 

18Inter-laboratory validation of a thin film microextraction technique for determination of pesticides in surface water samples

H Piri-Moghadam, E Gionfriddo, A Rodriguez-Lafuente, JJ Grandy, H L Lord, T Obal, J Pawliszyn

Analytica Chimica Acta 964, 74-84

 

17- New generation of solid-phase microextraction coatings for complementary separation approaches: a step toward comprehensive metabolomics and multiresidue Analyses in Complex Matrices

E Gionfriddo, E Boyacı, J Pawliszyn

Analytical Chemistry 89 (7), 4046-4054

 

16- Insights into the effect of the PDMS-layer on the kinetics and thermodynamics of analyte sorption onto the matrix-compatible solid phase microextraction coating

ÉA Souza-Silva, E Gionfriddo, MN Alam, J Pawliszyn

Analytical Chemistry 89 (5), 2978-2985

 

15- Towards on-site analysis of complex matrices by solid-phase microextraction-transmission mode coupled to a portable mass spectrometer via direct analysis in real time

GA Gómez-Ríos, T Vasiljevic, E Gionfriddo, M Yu, J Pawliszyn

Analyst 142 (16), 2928-2935

2016

14- Coupling solid phase microextraction to complementary separation platforms for metabotyping of E. coli metabolome in response to natural antibacterial agents

F Mousavi, E Gionfriddo, E Carasek, EA Souza-Silva, J Pawliszyn

Metabolomics 12 (11), 169

 

13- A facile and fully automated on-fiber derivatization protocol for direct analysis of short-chain aliphatic amines using a matrix compatible solid-phase microextraction coating

E Gionfriddo, A Passarini, J Pawliszyn

Journal of Chromatography A 1457, 22-28

 

12- Solid phase microextraction on-fiber derivatization using a stable, portable, and reusable pentafluorophenyl hydrazine standard gas generating vial

JJ Poole, JJ Grandy, GA Gómez-Ríos, E Gionfriddo, J Pawliszyn

Analytical Chemistry 88 (13), 6859-6866

 

11- Methodical evaluation and improvement of matrix compatible PDMS-overcoated coating for direct immersion solid phase microextraction gas chromatography (DI-SPME-GC)-based applications

ÉA Souza-Silva, E Gionfriddo, R Shirey, L Sidisky, J Pawliszyn

Analytica Chimica Acta 920, 54-62

2015

10- A critical review of the state of the art of solid-phase microextraction of complex matrices I. Environmental analysis

EA Souza-Silva, R Jiang, A Rodriguez-Lafuente, E Gionfriddo, J Pawliszyn

TrAC Trends in Analytical Chemistry 71, 224-235

 

9- A critical review of the state of the art of solid-phase microextraction of complex matrices II. Food analysis

ÉA Souza-Silva, E Gionfriddo, J Pawliszyn

TrAC Trends in Analytical Chemistry 71, 236-248

 

8- Headspace versus direct immersion solid phase microextraction in complex matrixes: Investigation of analyte behavior in multicomponent mixtures

E Gionfriddo, EA Souza-Silva, J Pawliszyn

Analytical Chemistry 87 (16), 8448-8456

2014

7- A fast and simple solid phase microextraction coupled with gas chromatography-triple quadrupole mass spectrometry method for the assay of urinary markers of glutaric acidemias

A Naccarato, E Gionfriddo, R Elliani, G Sindona, A Tagarelli

Journal of Chromatography A 1372, 253-259

 

6- Determination of hydrazine in drinking water: Development and multivariate optimization of a rapid and simple solid phase microextraction-gas chromatography-triple quadrupole mass spectrometry protocol

E Gionfriddo, A Naccarato, G Sindona, A Tagarelli

Analytica chimica acta 835, 37-45

 

5- Development of needle trap technology for on-site determinations: active and passive sampling

S Asl-Hariri, GA Gómez-Ríos, E Gionfriddo, P Dawes, J Pawliszyn

Analytical Chemistry 86 (12), 5889-5897

 

4- Simultaneous determination of benzothiazoles, benzotriazoles and benzosulfonamides by solid phase microextraction-gas chromatography-triple quadrupole mass spectrometry in environmental aqueous matrices and human urine

A Naccarato, E Gionfriddo, G Sindona, A Tagarelli

Journal of Chromatography A 1338, 164-173

 

3- Development of a simple and rapid solid phase microextraction-gas chromatography–triple quadrupole mass spectrometry method for the analysis of dopamine, serotonin and norepinephrine in human urine

A Naccarato, E Gionfriddo, G Sindona, A Tagarelli

Analytica chimica acta 810, 17-24

2012

2- A reliable solid phase microextraction-gas chromatography–triple quadrupole mass spectrometry method for the assay of selenomethionine and selenomethylselenocysteine in aqueous extracts: difference between selenized and not-enriched selenium potatoes

E Gionfriddo, A Naccarato, G Sindona, A Tagarelli

Analytica chimica acta 747, 58-66

2011

1- Multistage mass spectrometry in quality, safety and origin of foods

Aiello, D.; De Luca., D; Gionfriddo, E.; Naccarato, A.; Napoli, A.; Romano, E.; Russo, A.; Sindona, G.; Tagarelli, A.
European Journal of Mass Spectrometry 17 (1), 1-31

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